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Direct
Electrochemical Synthesis of the Chelates of a Novel Ligand: Salicylhydra-zone
of 2-(N-tosyl-amino)benzaldehyde (61k)
L.M. Blanco and B.I. Kharisov of Universidad Autónoma de Nuevo León
and A.S. Burlov, A.D. Garnovskii, L.I. Kuznetsova and I.S. Vasilchenko
of Rostov State University report the direct electrochemical synthesis
of metallic chelates from a new ligand system and compare the products
with those synthesized using conventional chemical methods.
Redox
Properties of Electron Transfer Metalloproteins (75k)
Adrian W. Bott of Bioanalytical Systems, Inc. discusses methods used
to study the electrochemical properties of electron transfer metalloproteins
and the results of those studies.
The
Microdialysis Shunt Probe: The Influence of Bile Salts on Recovery of
Caffeine and Phenolphthalein Glucuronide and Use of In Vitro Recovery
Data for Calibration In Vivo (123k)
Kathleen
Heppert and Malonne Davies of BAS Kansas show that bile salts can affect
the recovery of analytes through the microdialysis probe, interacting
with phenolphthalein glucuronide but not caffeine. The authors also
show that when bile salts are taken into account, in vitro calibration
of the probe can be used to calculate the in vivo analyte concentration
in bile..
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